Silica materials with wall-embedded nitroxides provide efficient polarization matrices for dynamic nuclear polarization NMR

Eric Besson; Fabio Ziarelli; Emily Bloch; Guillaume Gerbaud; Séverine Queyroy; Stéphane Viel; Stéphane Gastaldi

doi:10.1039/C6CC01809B

Journal articles

Silica materials with wall-embedded nitroxides provide efficient polarization matrices for dynamic nuclear polarization NMR

Eric Besson ¹ Fabio Ziarelli ² Emily Bloch ³ Guillaume Gerbaud ⁴ Séverine Queyroy ¹ Stéphane Viel ¹ Stéphane Gastaldi ¹

1 ICR - Institut de Chimie Radicalaire

2 FRSCM - Fédération des Sciences Chimiques de Marseille

3 MADIREL - Matériaux divisés, interfaces, réactivité, électrochimie

4 BIP - Bioénergétique et Ingénierie des Protéines

Abstract : Hybrid mesoporous silica materials with wall-embedded nitroxides are shown to efficiently polarize impregnated substrates in high-field dynamic nuclear polarization magic-angle spinning solid-state NMR experiments.

Document type :

Journal articles

Domain :

Chemical Sciences / Theoretical and/or physical chemistry

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https://hal-amu.archives-ouvertes.fr/hal-01415149
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Submitted on : Monday, December 12, 2016 - 6:49:00 PM
Last modification on : Tuesday, December 14, 2021 - 8:42:06 AM

Silica materials with wall-embedded nitroxides provide efficient polarization matrices for dynamic nuclear polarization NMR

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Silica materials with wall-embedded nitroxides provide efficient polarization matrices for dynamic nuclear polarization NMR

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